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Registro Completo |
Biblioteca(s): |
Embrapa Recursos Genéticos e Biotecnologia. |
Data corrente: |
28/03/2009 |
Data da última atualização: |
07/05/2024 |
Tipo da produção científica: |
Boletim de Pesquisa e Desenvolvimento |
Autoria: |
FARIAS, M. P. de; NÁVIA, D.; ARAÚJO, A. C. G. |
Afiliação: |
MARCELO PICANÇO DE FARIAS; DENISE NÁVIA MAGALHÃES FERREIRA, EMBRAPA RECURSOS GENÉTICOS E BIOTECNOLOGIA; ANA CLAUDIA GUERRA DE ARAÚJO, EMBRAPA RECURSOS GENÉTICOS E BIOTECNOLOGIA. |
Título: |
Adaptação de protocolo para visualizaçâo de caracteres taxonômicos do ácaro eriofídeo Aceria tosichella, Keifer em microscopia eletrônica de varredura. |
Ano de publicação: |
2008 |
Fonte/Imprenta: |
Brasília: Embrapa Recursos Genéticos e Biotecnologia, 2008. |
Páginas: |
12 p. |
Série: |
(Embrapa Recursos Genéticos e Biotecnologia. Boletim de Pesquisa e Desenvolvimento, 238). |
Idioma: |
Português |
Palavras-Chave: |
Keifer. |
Thesagro: |
Ácaro; Microscopia Eletrônica; Taxonomia. |
Thesaurus Nal: |
Aceria tosichella. |
Categoria do assunto: |
-- |
URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/CENARGEN-2009-09/31589/3/bp238_1208.pdf
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Marc: |
LEADER 00767nam a2200205 a 4500 001 1191238 005 2024-05-07 008 2008 bl uuuu u0uu1 u #d 100 1 $aFARIAS, M. P. de 245 $aAdaptação de protocolo para visualizaçâo de caracteres taxonômicos do ácaro eriofídeo Aceria tosichella, Keifer em microscopia eletrônica de varredura.$h[electronic resource] 260 $aBrasília: Embrapa Recursos Genéticos e Biotecnologia$c2008 300 $a12 p. 490 $a(Embrapa Recursos Genéticos e Biotecnologia. Boletim de Pesquisa e Desenvolvimento, 238). 650 $aAceria tosichella 650 $aÁcaro 650 $aMicroscopia Eletrônica 650 $aTaxonomia 653 $aKeifer 700 1 $aNÁVIA, D. 700 1 $aARAÚJO, A. C. G.
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Embrapa Recursos Genéticos e Biotecnologia (CENARGEN) |
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Registro Completo
Biblioteca(s): |
Embrapa Pecuária Sudeste. |
Data corrente: |
14/07/2011 |
Data da última atualização: |
27/07/2022 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Circulação/Nível: |
B - 3 |
Autoria: |
DONATI, G. L.; ROSINI, F.; NOGUEIRA, A. R. de A.; NOBREGA, J. A. |
Afiliação: |
GEORGE L. DONATI, UFSCar/SÃO CARLOS, SP; FABIANA ROSINI, UFSCar/SÃO CARLOS, SP; ANA RITA DE ARAUJO NOGUEIRA, CPPSE; JOAQUIM A. NÓBREGA, UFSCar/SÃO CARLOS, SP. |
Título: |
Focused-microwave-unduced combustion: investigation of KCIO3 thermal decomposition as O2 source. |
Ano de publicação: |
2011 |
Fonte/Imprenta: |
Analytical Methods, v. 3, n. 7, p. 1688-1691, 2011. |
DOI: |
https://doi.org/10.1039/C1AY05154G |
Idioma: |
Inglês |
Conteúdo: |
Potassium chlorate is proposed here as a chemical source of O2 in focused-microwave-induced combustion. The thermal decomposition of this compound generates enough O2 to maintain the combustion and participate in gas phase reactions responsible for HNO3 regeneration. An animal feed concentrate is the reference material and test sample used. Important parameters such as HNO3 concentration in the absorbing solution, volumes of igniting and oxidizing agents added to the sample, and microwave total incidence time were evaluated using a multivariate approach. The method efficiency was evaluated by determining both the residual carbon content (RCC) in the digestates and the recoveries of Ca, Mg, Mn, P and Zn using inductively coupled plasma optical emission spectrometry. Recoveries in the 82.3?102% range were obtained for all elements studied using 5 mL of an absorbing solution with 5.0 mol L?1 of HNO3, and adding 110 ?L of NH4NO3 6.0 mol L?1 plus 140 ?L of KClO3 0.5 mol L?1 to the solid sample, in a 7 min digestion program. A RCC value of 20% and a final acid concentration of 0.19 mol L?1 were obtained in the combustion of 100 mg of sample under optimized conditions. These preliminary results show the capabilities of a simple, inexpensive method with potential for different applications in procedures taking no longer than a few minutes. It is compatible with commercially available focused-microwave systems and requires no instrumental modification for its implementation. |
Palavras-Chave: |
Focused microwave unduced. |
Categoria do assunto: |
W Química e Física |
Marc: |
LEADER 02078naa a2200181 a 4500 001 1895884 005 2022-07-27 008 2011 bl uuuu u00u1 u #d 024 7 $ahttps://doi.org/10.1039/C1AY05154G$2DOI 100 1 $aDONATI, G. L. 245 $aFocused-microwave-unduced combustion$binvestigation of KCIO3 thermal decomposition as O2 source.$h[electronic resource] 260 $c2011 520 $aPotassium chlorate is proposed here as a chemical source of O2 in focused-microwave-induced combustion. The thermal decomposition of this compound generates enough O2 to maintain the combustion and participate in gas phase reactions responsible for HNO3 regeneration. An animal feed concentrate is the reference material and test sample used. Important parameters such as HNO3 concentration in the absorbing solution, volumes of igniting and oxidizing agents added to the sample, and microwave total incidence time were evaluated using a multivariate approach. The method efficiency was evaluated by determining both the residual carbon content (RCC) in the digestates and the recoveries of Ca, Mg, Mn, P and Zn using inductively coupled plasma optical emission spectrometry. Recoveries in the 82.3?102% range were obtained for all elements studied using 5 mL of an absorbing solution with 5.0 mol L?1 of HNO3, and adding 110 ?L of NH4NO3 6.0 mol L?1 plus 140 ?L of KClO3 0.5 mol L?1 to the solid sample, in a 7 min digestion program. A RCC value of 20% and a final acid concentration of 0.19 mol L?1 were obtained in the combustion of 100 mg of sample under optimized conditions. These preliminary results show the capabilities of a simple, inexpensive method with potential for different applications in procedures taking no longer than a few minutes. It is compatible with commercially available focused-microwave systems and requires no instrumental modification for its implementation. 653 $aFocused microwave unduced 700 1 $aROSINI, F. 700 1 $aNOGUEIRA, A. R. de A. 700 1 $aNOBREGA, J. A. 773 $tAnalytical Methods$gv. 3, n. 7, p. 1688-1691, 2011.
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